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Beilstein J. Org. Chem. 2019, 15, 780–788, doi:10.3762/bjoc.15.74
Graphical Abstract
Scheme 1: Approach of the direct azologization of reported [60,61] serotonin 5-HT3R antagonists via replacement of a...
Scheme 2: Synthesis of the differently substituted quinoxaline azobenzene derivatives 5a and 5b via Baeyer [62]–M...
Scheme 3: Synthesis of the methoxy-substituted quinoxaline derivative 12a via diazotization [66-69].
Scheme 4: General procedure for the synthesis of purine- and thienopyrimidine-substituted arylazobenzenes and...
Scheme 5: Synthesis of the thiomethyl-linked purine azobenzene 23 [62,63,72-74].
Scheme 6: Synthesis of the amide-linked azobenzene purine 28 [62,63,75-77].
Figure 1: UV–vis absorption spectra measured at 50 µM in DMSO. Left: purine derivative 16c; right: azo-extend...
Figure 2: On the left panel representative traces of currents induced by the application of 3 µM 5HT (black t...